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| - | **Overview** | + | ==== Overview |
| - | + | ||
| - | The Merlin AutoGC Xplorer (MAX) is a cloud-based database designed to ingest data generated by chromatographic equipment deployed into EPA Photochemical Assessment Monitoring Sites (PAMS) which are collecting and analyzing hourly concentrations of up to 60 volatile organic compounds (VOC). | + | The Merlin AutoGC Xplorer (**MAX**) is a cloud-based database designed to ingest data generated by chromatographic equipment deployed into EPA Photochemical Assessment Monitoring Sites (**PAMS**) which are collecting and analyzing hourly concentrations of up to 60 volatile organic compounds (**VOC**). MAX is a Structured Query Language (**SQL**) database of the data which includes the necessary information to allow users to view and graphically evaluate the hourly concentration data from these sites. |
| Orsat, LLC has developed and designed MAX to accommodate data originating from either PerkinElmer Ozone Precursor systems or Agilent systems using Markes International pre-concentration sampling system. | Orsat, LLC has developed and designed MAX to accommodate data originating from either PerkinElmer Ozone Precursor systems or Agilent systems using Markes International pre-concentration sampling system. | ||
| - | **Features** | + | ==== Features ==== |
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| + | The PAMS AutoGC systems collect not only hourly ambient air data but also have Quality Control samples which are outlined in the EPA PAMS Technical Assistance Guidance document (**TAD**). | ||
| + | === Quality Control Sample Types === | ||
| + | - Calibration Verification Standard (CVS) or Continuing Calibration Verification (CCV) Standard | ||
| + | * Required daily | ||
| + | * Used to confirm system response daily; recoveries generally ± 30% specified in the Network configuration | ||
| + | - System Blank (SB) or Method Blank | ||
| + | * Required daily | ||
| + | * Used to determine concentrations of target compounds which may be contributed by the analytical system | ||
| + | - Laboratory Calibration Standard (LCS) or Second Source Calibration Verification (SSCV) Standard | ||
| + | * Required weekly | ||
| + | * Used to confirm original calibration by reference. | ||
| + | - Retention Time Standard (RTS) | ||
| + | * Required weekly | ||
| + | * Used to verify correct target identification by retention time windows in method. | ||
| + | |||
| + | | ||
| + | === Format for Incoming Data - ASCII Text === | ||
| + | The output format for data generated by the analytical data system must adhere to a specific ASCII text format to enable MAX to be able to correctly interpret and store the data. Orsat has generated output formats for both the Totalchrom and EZChrom data systems. | ||
| + | |||
| + | * Instrument Name - (Format " | ||
| + | * Filename - specific format (see File Naming) | ||
| + | * Acquisition Time - the time the analytical data collection started. | ||
| + | * Process Date and time- the time the data file was generated | ||
| + | * Sample Name, generally Blank, Standard, Ambient Air, IQ-RTS, CS-LCS | ||
| + | * Instrument Name | ||
| + | * Instrument method filename | ||
| + | * Sequence filename | ||
| + | * Peak Details | ||
| + | * Component Name | ||
| + | * Amount in ppbC | ||
| + | * Retention time | ||
| + | * Peak Area | ||
| + | |||
| + | MAX was designed to identify the QC control samples by using a specific file naming paradigm. | ||
| + | |||
| + | Filename structure.png | ||
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| + | ==== Network and Site Configuration ==== | ||
| + | |||
| + | In order to allow the evaluation of these QC samples each data set or //Site// has a definition which incorporates configuration parameters for the //Network// which defines information about incoming data such as a list of target VOCs, which targets will be in the QC samples and their concentrations and control limits. | ||
| + | === Information Required for Network Configuration === | ||
| + | |||
| + | - Units (default is ppbC) | ||
| + | - How Lost data will be displayed | ||
| + | - How zero values will be displayed | ||
| + | - Total Blank Maximum value | ||
| + | - List of Target Compounds by Channel | ||
| + | - List of Target Compounds in each of the required QC samples (LCS, CVS, RTS, Blank and MDL by channel including required limits or thresholds | ||
| + | - List of applicable Null, Qualifier and Inform Flags available for use in AQS files. | ||
| + | |||
| + | Each Site also has unique information to identify it in the database. | ||
| - | The PAMS AutoGC systems collect not only hourly ambient air data but also have Quality Control samples which are outlined in the EPA PAMS Technical Assistance Guidance document (TAD). | + | === Information Required |
| + | - Site name (defined in the incoming ASCII text file as " | ||
| + | - Type - designation of data system generating the data, PerkinElmer or EZChrom | ||
| + | - Minimum display value - generally 0 | ||
| + | - Network assigned to the site | ||
| + | - AQS number assigned to the site | ||
| + | - POC if necessary | ||
| + | - Short name - user entered text field | ||
| + | - Formal name - user entered text field | ||
| + | - Address, City and Zipcode | ||
| + | - Latitude and Longitude | ||
| + | - UTC offset | ||
| + | - CAMS code (if available) | ||
| + | - Interval, units code and method codes required for AQS file generation | ||
| + | ---- | ||
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| * | * | ||
| + | ---- | ||
| **References** | **References** | ||